Stepwise collapse of a giant pore metal–organic framework ...
Thermogravimetric analysis (TGA) was used to compare the effect of ball milling upon thermal stability, and in particular to examine the effect of defect incorporation. The TGA traces of crystalline MIL-100 and the ball-milled materials exhibited three characteristic mass losses, consistent with previous reports [ Fig. 5a ]. 28 Firstly, at ...